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1 article(s) from Allen, Ray W. K.

Continuous-flow Heck synthesis of 4-methoxybiphenyl and methyl 4-methoxycinnamate in supercritical carbon dioxide expanded solvent solutions

Phei Li Lau,
Ray W. K. Allen and
Peter Styring

Beilstein J. Org. Chem. 2013, 9, 2886–2897, doi:10.3762/bjoc.9.325

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Graphical Abstract

Scheme 1: General Heck reaction showing the possible isomers that can be produced.

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Figure 1: Schematic diagram of the stirred autoclave reactor. Pickel’s pump NWA PM101 was used to achieve sup...

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Figure 2: Schematic diagram of the continuous flow system. The reactor shown is the 3.9 mm i.d. PFR. For the ...

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Figure 3: Total conversion of 4-iodoanisole as a function of reactor run time for three reaction temperatures....

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Figure 4: Total conversion of 4-iodoanisole at 155 °C and 200 bar as a function of reactor run time for diffe...

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Figure 5: Total conversion of 4-iodoanisole as a function of reactor run time at 145 °C and at 200 (●) and 25...

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Figure 6: Conversion of 4-iodoanisole to methyl 4-methoxycinnamate (●) at 155 °C and 200 bar as a function of...

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Figure 7: Comparison of conversion as a function of reactor run time for the reaction of methyl acrylate in t...

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Figure 8: TOF values for the 1 mm (ο) and 3.9 mm (●) PFRs at a total flow rate of 0.12 mL min⁻¹, 155 °C and 2...

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Figure 9: Turnover frequencies of the Heck reactions at 155 °C using styrene (ο) as combined isomeric product...

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Published 17 Dec 2013

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